HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloro-2-butene → (6-benzoyl-2-pyridyl)methyl 2-[N-(2-chloro-2-propenyl)amino]-3-methylbutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloro-2-butene | HCID 13556 | — |
| Reactant | 3-Bromo-2-chloroprop-1-ene | HCID 235121 | — |
| Reactant | (6-Benzoyl-2-pyridyl)methyl 2-amino-3-methylbutanoate | HCID 20461184 | — |
| Product | (6-benzoyl-2-pyridyl)methyl 2-[N-(2-chloro-2-propenyl)amino]-3-methylbutanoate | HCID 20461185 | — |
| Product | (6-benzoyl-2-pyridyl)methyl 2-[N-(3-chloro-2-butenyl)amino]-3-methylbutanoate | HCID 54537610 | — |
Reaction Steps
Using the method of Example 2, (6-benzoyl-2-pyridyl)methyl 2-amino-3-methylbutanoate is reacted with each of 2-chloro-2-propen-1-yl bromide and 3-chloro-2-buten-1-yl chloride to yield (6-benzoyl-2-pyridyl)methyl 2-[N-(2-chloro-2-propenyl)amino]-3-methylbutanoate and (6-benzoyl-2-pyridyl)methyl 2-[N-(3-chloro-2-butenyl)amino]-3-methylbutanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04447613 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-2b493799415144a5a9877d7c4423cd41 |
| Source note | uspto-grants-1984_05 |