HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzoic Acid → 2,3-Dihydro-2-[[-(4-methoxybenzoyl)-1-piperazinyl]methyl]-2,4,6,7-tetramethyl-5-benzofuranamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzoic Acid | HCID 7478 | — |
| Reactant | 2,3-Dihydro-2,4,6,7-tetramethyl-2-[(1-piperazinyl)methyl]-5-benzofuranamine | HCID 21997779 | — |
| Product | 2,3-Dihydro-2-[[-(4-methoxybenzoyl)-1-piperazinyl]methyl]-2,4,6,7-tetramethyl-5-benzofuranamine | HCID 22110975 | 67% |
Reaction Steps
Using 2,3-dihydro-2,4,6,7-tetramethyl-2-[(1-piperazinyl)methyl]-5-benzofuranamine and p-anisic acid, the procedure of Example 10, presented hereinafter, was otherwise followed to provide the title compound. Yield 67%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172085B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-77a50fbee5354e05ac0f3816662a9eaf |
| Source note | uspto-grants-2001_01 |