HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Butyn-2-ol → Undec-8-en-3-yne-2,5-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Butyn-2-ol | HCID 16239 | — |
| Reactant | Hept-4-enal | HCID 71590 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Undec-8-en-3-yne-2,5-diol | HCID 123300045 | — |
Reaction Steps
But-3-yn-2-ol was added into a solution of ethyl magnesium bromide (EtMgBr) in tetrahydrofuran (THF). Hept-4-enal was then dropped into the mixture at room temperature and aged for 2 hours. The rush over process provided the product undec-8-en-3-yne-2,5-diol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09441185B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-031d4fef6cf0407a9a44ce165221682a |
| Source note | uspto-grants-2016_09 |