HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → 2-(4-Bromobutyl)-3,4-dihydro-2-(3,4-dimethoxyphenyl)-4-methyl-3-oxo-2H-1,4-benzothiazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | HCID 14244692 | HCID 14244692 | — |
| Product | 2-(4-Bromobutyl)-3,4-dihydro-2-(3,4-dimethoxyphenyl)-4-methyl-3-oxo-2H-1,4-benzothiazine | HCID 20143035 | 67.2% |
Reaction Steps
3,4-Dihydro-2-(3,4-dimethoxyphenyl)-4-methyl-3-oxo-2H-1,4-benzothiazine (5.0 g) and 1,4-dibromobutane (10.3 g) are treated by the similar method as in Example 12 to give 4.8 g (66.9%) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04739050 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-1466abe5a8a746fc9ad5ca1adb2bfca9 |
| Source note | uspto-grants-1988_04 |