HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyloctylamine → HCID 178419187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyloctylamine | HCID 16224 | — |
| Reactant | borane;N,N-diethylethanamine | HCID 264094 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 178419187 | HCID 178419187 | 89% |
Reaction Steps
Octyldimethylamine (20.4 grams; 0.130 mole) was heated with triethylamine borane (1.9 grams; 0.130 mole) at reflux temperature until 12.8 grams (98%) of triethylamine had been collected in a cold trap. The reaction residue was distilled at reduced pressure to give N-octyl-N,N-dimethylamine borane boiling at 98°-100° C./0.9 mm. Hg. (19.6 grams; 89% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04740504 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-d602c547b2d447c5a70a59f83b9251c5 |
| Source note | uspto-grants-1988_04 |