HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21713540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,1,2,3,3-Pentamethylindan | HCID 14549 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1H-Indene, octahydro-1,1,2,3,3-pentamethyl- | HCID 118537 | — |
| Product | HCID 21713540 | HCID 21713540 | — |
Reaction Steps
prepared according to the disclosure of U.S. Pat. No. 4,902,840 issued on Feb. 20, 1990, the specification for which is incorporated herein by reference; 20% 1,1,2,3,3-pentamethylindane and 35% hexahydro-1,1,2,3,3-pentamethylindane is heated to 150° C. Hydrogen chloride gas evolves and is passed through a caustic soda scrubber. This solution is then washed with a 5% aqueous sodium hydroxide solution, dried over anhydrous magnesium sulfate and used without further purification in the next step, the carrying out of an oxo-reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271193B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-0c5e48e985044412bfd33fa090a3cb16 |
| Source note | uspto-grants-2001_08 |