HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178429957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Aminoantipyrine | HCID 2151 | — |
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Catalyst | HCID 178511488 | HCID 178511488 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178429957 | HCID 178429957 | — |
Reaction Steps
10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of 3-chlorophenol in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582123B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-90d47fe86fee49e6960a89f297290853 |
| Source note | uspto-grants-2009_09 |