HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furan-2-sulfonyl Chloride → HCID 53492428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furan-2-sulfonyl Chloride | HCID 2795072 | — |
| Reactant | 5,6-difluoro-N1-(2-fluoro-4-iodophenyl)benzene-1,2-diamine | HCID 59386306 | — |
| Product | HCID 53492428 | HCID 53492428 | — |
Reaction Steps
According to the general procedure B, 5,6-difluoro-N1-(2-fluoro-4-iodophenyl)benzene-1,2-diamine was reacted with furan-2-sulfonyl chloride to obtain the title compound. 1H NMR (300 MHz, CDCl3): δ 7.53 (br s, D2O exchangeable, 1H), 7.38 (dd, J=1.8 & 10.5 Hz, 1H), 7.30 (d, J=8.4 Hz, 1H), 7.21 (d, J=3.0 Hz, 1H), 6.96 (dd, J=8.7 & 16.5 Hz, 1H), 6.87 (ddd, J=1.8, 5.1 & 9.0 Hz, 1H), 6.53 (dd, J=1.8 & 3.6 Hz, 1H), 6.44 (dt, J=5.1, 8.7 & 13.8 Hz, 1H), 6.22 (br s, D2O exchangeable, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08829052B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-30dc24649bbe46ffaf4fe1045cff34b1 |
| Source note | uspto-grants-2014_09 |