Bis(cyclohexylammonium)sulfate → HCID 131726955, compound

HRID 747589

Reaction equation

HRID 747589 reaction equation
[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[NH4+].[NH4+].S(O)(O)(=O)=[O:9].C1(N)CCCCC1.C1(N)CCCCC1.S(O)(O)(=O)=[O:28].[CH:32]1([NH:38][CH:39]2[CH2:44][CH2:43][CH2:42][CH2:41][CH2:40]2)[CH2:37][CH2:36][CH2:35][CH2:34][CH2:33]1.[CH:45]1([NH:51][CH:52]2[CH2:57][CH2:56][CH2:55][CH2:54][CH2:53]2)[CH2:50][CH2:49][CH2:48][CH2:47][CH2:46]1>>[S:1]([OH:5])([OH:4])(=[O:3])=[O:2].[CH:39]1([N:38]([CH:32]2[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37]2)[OH:28])[CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]1.[CH:52]1([N:51]([CH:45]2[CH2:46][CH2:47][CH2:48][CH2:49][CH2:50]2)[OH:9])[CH2:53][CH2:54][CH2:55][CH2:56][CH2:57]1

Participants

4

Reactant 3

HCID 159837Bis(cyclohexylammonium)sulfateHCID 6097028Ammonium SulfateHCID 131726956HCID 131726956, compound

Product 1

HCID 131726955HCID 131726955, compound

Procedure

It can be seen from the NMR spectrum which is then measured that DCHAS has been formed. Traces of oxime, ammonium sulfate, CHAS, cyclohexylamine hemisulfate and dicyclohexylamine hemisulfate can be discerned as impurities in the NMR spectrum.

Workup

  1. customhas been formed

Sources & evidence

ORD record
ord-b2308dba9c2b4fe8aaa6de3fb1883cc3
Source dataset
uspto-grants-2008_07
Patent number
US07396959B2

Linked notes

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