HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → n,n'-Bis-((e)-3-(2-methoxyphenyl)-2-propenyl)piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methoxy-cinnamylalcohol | HCID 53401658 | — |
| Product | n,n'-Bis-((e)-3-(2-methoxyphenyl)-2-propenyl)piperazine | HCID 19694161 | — |
Reaction Steps
2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723465 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-d2aea31453084c8dba037f866c0833b5 |
| Source note | uspto-grants-1998_03 |