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3-[(5-Hydroxymethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester → 3-[(5-Hydroxymethyl-furan-2-ylmethyl)-amino]-phthalic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-[(5-Hydroxymethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester | HCID 21040137 | — |
| 反応物 | 3-(2-Methoxy-ethylamino)-phthalic acid | HCID 21988519 | — |
| 生成物 | 3-[(5-Hydroxymethyl-furan-2-ylmethyl)-amino]-phthalic acid | HCID 21988584 | — |
反応手順
3-[(5-Hydroxymethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester (0.97 g, 3.04 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091353B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-22f8c12012f2426eaa164d66c497f0db |
| 出典メモ | uspto-grants-2006_08 |