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3-oxo-3,4-dihydro-2H-1,4-benzoxazine-6-carbaldehyde → HCID 178489236、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-oxo-3,4-dihydro-2H-1,4-benzoxazine-6-carbaldehyde | HCID 10773638 | — |
| 反応物 | 4-Methoxy-1,3-benzothiazole | HCID 12631858 | — |
| 反応物 | HCID 178502731 | HCID 178502731 | — |
| 生成物 | HCID 178489236 | HCID 178489236 | — |
反応手順
The title compound was prepared according to the same protocol as that described for example 1, steps 1.a to 1.c, using 4-methoxy-benzothiazole (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-6-carbaldehyde (0.3 mmol). An orange solid (74 mg) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07981886B2 |
| 出典データセット | uspto-grants-2011_07 |
| ORD ID | ord-a7ce56630155459286ed9c6b10670c7e |
| 出典メモ | uspto-grants-2011_07 |