化工社化工社 化学情報印刷レポート · 研究参考用
Formamide → 7-Methyl-2,3-dihydroisoquinolin-3-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formamide | HCID 713 | — |
| 反応物 | 2-(4-Methylphenyl)acetyl chloride | HCID 2760634 | — |
| 反応物 | N-formyl-2-(p-methylphenyl)-acetamide | HCID 21541248 | — |
| 反応物 | N-formyl-N-methyl-2-phenyl-acetamide | HCID 21541252 | — |
| 生成物 | 7-Methyl-2,3-dihydroisoquinolin-3-one | HCID 21541258 | — |
反応手順
The N-formyl-2-(p-methylphenyl)-acetamide (m.p. 144°-146°C.) used as starting material was prepared from formamide and 4-methyl-phenyl-acetyl chloride in the manner described in Example 2 for the preparation of N-formyl-N-methyl-2-phenyl-acetamide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03954771 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-93e36159cab04c1d972f97e0de8a5795 |
| 出典メモ | uspto-grants-1976_05 |