化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → Diethyl 3-(4-chlorophenyl)-2-isoxazolin-5-ylmethylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Chlorosuccinimide | HCID 31398 | — |
| 反応物 | 4-Chloro-benzaldehyde oxime | HCID 219158 | — |
| 反応物 | Diethyl allylphosphonate | HCID 573014 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Diethyl 3-(4-chlorophenyl)-2-isoxazolin-5-ylmethylphosphonate | HCID 20062407 | 104.5% |
反応手順
Preparation is carried out as in Example 1 from 23.34 g of 4-chlorobenzaldoxime, 22 g of N-chlorosuccinimide, 29.5 g of diethyl allylphosphonate and 22.9 ml of triethylamine in dichloromethane and provides 52 g of oily product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05006515 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-abc093e2107b434cbc94fb24708993c0 |
| 出典メモ | uspto-grants-1991_04 |