化工社化工社 化学情報印刷レポート · 研究参考用
2-Aminopropanol → 4-Methyl-2-undecyl-2-oxazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Aminopropanol | HCID 5126 | — |
| 反応物 | Dodecanenitrile | HCID 17092 | — |
| 触媒 | Cadmium acetate, dihydrate | HCID 6537495 | — |
| 溶媒 | 1-Butanol | HCID 263 | — |
| 生成物 | 4-Methyl-2-undecyl-2-oxazoline | HCID 14651791 | 92% |
反応手順
10.9 g (60 mmoles) of undecyl cyanide was treated with 5 g (66.6 mmoles) of DL-2-amino-1-propanol in presence of 400 mg (1.5 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 13.2 g (92%) of product was obtained on distillation at 115°-117° C./1-1.5 mm Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05030629 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-8fcaecc793d94a60abd145079f17f86a |
| 出典メモ | uspto-grants-1991_07 |