化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylpropylenediamine → 4,4-Dimethyl-2-undecyl-2-imidazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylpropylenediamine | HCID 13128 | — |
| 反応物 | Dodecanenitrile | HCID 17092 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | 4,4-Dimethyl-2-undecyl-2-imidazoline | HCID 178442809 | 78% |
反応手順
18.31 g (100 mmoles) of undecyl cyanide, 11 g (125 mmoles) of 1,2-diamino-2-methylpropane and 0.5 ml of carbon disulfide were heated at 125° C. for 24 hrs. and then worked up as under Example 23. Distillation at reduced pressure gave 19.66 g (78%) of the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05030629 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-5033a1029d18466ba36806c9e6bafe4f |
| 出典メモ | uspto-grants-1991_07 |