関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Octacosanoic acid | HCID 10470 | — |
| 反応物 | Diglycerin | HCID 42953 | — |
| 反応物 | Tin atom | HCID 5352426 | — |
| 生成物 | Diglycerol sesquimontanate | HCID 131716646 | — |
反応手順
112 g diglycerol (0.67 mole), 400 g montanic acid (1.0 mole) and 0.4 g tin powder were heated to 200° C. as in Example 1 with application of a gentle vacuum. The vacuum was increased to 24 mbar over a period of 3.4 h. The product had an acid value of approximately 1. A brown colored hard wax having a dropping point of 81° C. was obtained after cooling to 100° C., bleaching and filtering.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04962145 |
|---|
| 出典データセット | uspto-grants-1990_10 |
|---|
| ORD ID | ord-8242717f30c14ddebc0995dac6a68de3 |
|---|
| 出典メモ | uspto-grants-1990_10 |
|---|
