関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Styrene | HCID 7501 | — |
| 反応物 | Ethoxydimethylsilane | HCID 61772 | — |
| 触媒 | Platinum | HCID 23939 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Phenethyldimethylethoxysilane | HCID 54188620 | 27% |
反応手順
Comparative Example 1. (Reaction between Styrene and Dimethylethoxysilane) A glass tube was filled with 312 mg of styrene and 312 mg of dimethylethoxysilane. The contents were combined with 1 μL of a toluene solution of a complex of divinylsiloxane and 0-valence platinum (platinum content: 0.4 Wt. %). The tube was sealed with Teflon tape and was heated for 30 minutes in an oil bath at 41° C. After cooling, the product was subjected to GC analysis. The analyses confirmed that the conversion of styrene was 36% and that phenethyldimethylethoxysilane was produced at a yield of 27%. The yield of (α-methylbenzyl)dimethylethoxysilane was 8.5%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06060620 |
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| 出典データセット | uspto-grants-2000_05 |
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| ORD ID | ord-bb1ecc69861a4a45b877fa71c023ca0c |
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| 出典メモ | uspto-grants-2000_05 |
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