2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione → HCID 88807735、化合物

HRID 1112016

反応式

HRID 1112016 の反応式
[C:1]([OH:4])(=[S:3])[CH3:2].[CH:5]1([S:11]N2C(=O)C3=CC=CC=C3C2=O)[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1>C1C=CC=CC=1>[C:1]([S:3][S:11][CH:5]1[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1)(=[O:4])[CH3:2]

参加物

4

反応物 2

HCID 287772-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dioneHCID 178418634HCID 178418634、化合物

生成物 1

HCID 88807735HCID 88807735、化合物収率 98%

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

Thioacetic acid, 0.444 moles, 3.35 grams, is reacted with N-(cyclohexylthio)phthalimide in 100 ml of benzene and the product recovered following a procedure similar to Example 11. Acetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams). Analysis gives 51.27%C, 7.41%H and 31.78%S compared to 50.6%C, 7.38%H and 33.7%S calculated for C8H14OS2.

後処理

  1. customthe product recovered
  2. customAcetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams)
  3. customAnalysis gives 51.27%C, 7.41%H and 31.78%S

出典と根拠

ORDレコード
ord-7ebf498ea6c84e2ea5e8f1d9bf6fbb7e
出典データセット
uspto-grants-1978_10
特許番号
US04119780

関連ノート

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