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HRID 1163913作成日:2026年10月23日

N,N-Diphenylhydrazine → N-Ethylcarbazole-3-carbaldehyde diphenylhydrazone

https://huagongshe.com/ja/reaction/1163913

反応式

関与物質

役割名称HCID仕込み量
反応物N,N-DiphenylhydrazineHCID 10739—
反応物9-ethyl-9H-carbazole-3-carbaldehydeHCID 82055—
溶媒EthanolHCID 702—
生成物N-Ethylcarbazole-3-carbaldehyde diphenylhydrazoneHCID 175429—

反応手順

1,1-diphenylhydrazine and N-ethylcarbazole-3-carbaldehyde were reacted in ethanol at room temperature to obtain N-ethylcarbazole-3-carbaldehyde diphenylhydrazone with melting point of 160.2°-160.5° C., and 60 parts of this hydrazone compound and 100 parts of a polyester (Vylon 200 by Toyobo Co., Ltd.) were dissolved in 450 parts of tetrahydrofuran to prepare a coating solution. Then selenium was vacuum evaporated on a 10 μm thick aluminum foil laminated on a 75 μm thick polyester film to form a charge generating layer with thickness of approximately 0.3 μm, and to this layer was applied the above-said coating solution by a film applicator and dried to form a 20 μm thick charge transporting layer. In this way, there was obtained a double-layer type electrophotographic plate.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04367273
出典データセットuspto-grants-1983_01
ORD IDord-eef9d805676f44cc89f89adc154effdf
出典メモuspto-grants-1983_01