関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N,N-Diphenylhydrazine | HCID 10739 | — |
| 反応物 | 9-ethyl-9H-carbazole-3-carbaldehyde | HCID 82055 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-Ethylcarbazole-3-carbaldehyde diphenylhydrazone | HCID 175429 | — |
反応手順
1,1-diphenylhydrazine and N-ethylcarbazole-3-carbaldehyde were reacted in ethanol at room temperature to obtain N-ethylcarbazole-3-carbaldehyde diphenylhydrazone with melting point of 160.2°-160.5° C., and 60 parts of this hydrazone compound and 100 parts of a polyester (Vylon 200 by Toyobo Co., Ltd.) were dissolved in 450 parts of tetrahydrofuran to prepare a coating solution. Then selenium was vacuum evaporated on a 10 μm thick aluminum foil laminated on a 75 μm thick polyester film to form a charge generating layer with thickness of approximately 0.3 μm, and to this layer was applied the above-said coating solution by a film applicator and dried to form a 20 μm thick charge transporting layer. In this way, there was obtained a double-layer type electrophotographic plate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04367273 |
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| 出典データセット | uspto-grants-1983_01 |
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| ORD ID | ord-eef9d805676f44cc89f89adc154effdf |
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| 出典メモ | uspto-grants-1983_01 |
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