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Sulfuric Acid → 2-Anilino-4-methyl-6-(1-propynyl)pyrimidine sulfate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Mepanipyrim | HCID 86296 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-Anilino-4-methyl-6-(1-propynyl)pyrimidine sulfate | HCID 15615498 | 75% |
反応手順
2-Anilino-4-methyl-6-(1-propynyl)pyrimidine (2.2 g) was dissolved in 100 ml of ethanol, and 2 ml of concentrated sulfuric acid was added thereto and stirred for 1 hour at room temperature. The crystals deposited were filtered, and dried to afford 2.4 g of 2-anilino-4-methyl-6-(1-propynyl)pyrimidine sulfate (yield 75%). Melting point: 192°-195° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04814338 |
| 出典データセット | uspto-grants-1989_03 |
| ORD ID | ord-b49530038cf74bd1a70d1733b5f02644 |
| 出典メモ | uspto-grants-1989_03 |