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(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester | HCID 67201113 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 67199974 | HCID 67199974 | — |
反応手順
The product of step b.) (2.0 g, 5.45 mmol) was stirred with 3% Pd/C (200 mg) in ethanol (20 mL) under H2 (1 atm) for 90 minutes. The reaction was filtered over celite and concentrated to dryness to give the sub-title compound as a brown oil. This compound was used in crude form without purification. MS: ESI (positive): 338 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07732618B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-87a849f7a0c44fe2bcd1487199a27e08 |
| 出典メモ | uspto-grants-2010_06 |