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HRID 15532作成日:2026年10月24日

(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974、化合物

https://huagongshe.com/ja/reaction/15532

反応式

関与物質

役割名称HCID仕込み量
反応物(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl esterHCID 67201113—
触媒PalladiumHCID 23938—
溶媒EthanolHCID 702—
生成物HCID 67199974HCID 67199974—

反応手順

The product of step b.) (2.0 g, 5.45 mmol) was stirred with 3% Pd/C (200 mg) in ethanol (20 mL) under H2 (1 atm) for 90 minutes. The reaction was filtered over celite and concentrated to dryness to give the sub-title compound as a brown oil. This compound was used in crude form without purification. MS: ESI (positive): 338 (M+H).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07732618B2
出典データセットuspto-grants-2010_06
ORD IDord-87a849f7a0c44fe2bcd1487199a27e08
出典メモuspto-grants-2010_06