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4-Pyridinecarboxaldehyde → 2-Methyl-6-[(pyridin-4-ylmethyl)-amino]-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| 反応物 | 6-Methylanthranilic acid | HCID 151210 | — |
| 生成物 | 2-Methyl-6-[(pyridin-4-ylmethyl)-amino]-benzoic acid | HCID 58989955 | — |
反応手順
Prepared by a similar procedure as described for preparation 1A, starting from 2-amino-6-methylbenzoic acid (Fluka) and pyridine-4-carbaldehyde. 13C-NMR (DMSO-d6) δ 170.4, 149.5, 149.3, 147.8, 138.5, 131.2, 121.9, 118.7, 115.8, 109.1, 45.1, 22.1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08034811B2 |
| 出典データセット | uspto-grants-2011_10 |
| ORD ID | ord-3ec030e59012453fbc61acb069187444 |
| 出典メモ | uspto-grants-2011_10 |