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Isoproterenone hydrochloride → HCID 20535341、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isoproterenone hydrochloride | HCID 2830496 | — |
| 反応物 | 2,3,4-Trimethylbenzoyl chloride | HCID 20437149 | — |
| 生成物 | HCID 20535341 | HCID 20535341 | — |
反応手順
Following the procedure described above in Example 58A but using 3,4-dihydroxyphenyl isopropylaminomethyl ketone hydrochloride instead of 3,4-dihydroxyphenyl tert-butylaminomethyl ketone hydrochloride and 2,3,4-trimethylbenzoyl chloride instead of isovaleryl chloride, there is obtained 3-hydroxy-4-(2,3,4-trimethylbenzoyloxy)phenyl isopropylaminomethyl ketone; and by interaction of this base with hydrochloric acid there is obtained the hydrochloride salt. When this hydrochloride is catalytically hydrogenated, using a procedure similar to that described above in Example 2B, there is obtained 3-hydroxy-4-(2,3,4-trimethylbenzoyloxy)-alpha-(isopropylaminomethyl)benzyl alcohol hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE030241 |
| 出典データセット | uspto-grants-1980_03 |
| ORD ID | ord-4ff684a163124ca2adf4c7a6beb45f41 |
| 出典メモ | uspto-grants-1980_03 |