関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Styrene | HCID 7501 | — |
| 反応物 | Dichloro(hexyl)silane | HCID 92038703 | — |
| 触媒 | HCID 178420539 | HCID 178420539 | — |
| 生成物 | n-Hexylphenethyldichlorosilane | HCID 20299100 | 91.1% |
反応手順
3.80 g (20.5 millimol) of n-hexyldichlorosilane, 2.00 g (19.2 millimol) of styrene, and 0.023 g (1.92×10-5 mol) of tetrakis(triphenylphosphine)platinum (O) were introduced into a flask and reacted with stirring by heating in an oil bath at 60° C. for 8 hours and then subjected to distillation under a reduced pressure to produce 5.6 g (17.5 millimol) of n-hexylphenethyldichlorosilane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04242272 |
|---|
| 出典データセット | uspto-grants-1980_12 |
|---|
| ORD ID | ord-4683dd3e1a49444ebbe1ea160db91666 |
|---|
| 出典メモ | uspto-grants-1980_12 |
|---|
