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Prop-2-en-1-yl 4-aminobenzoate → Allyl 4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Prop-2-en-1-yl 4-aminobenzoate | HCID 13075143 | — |
| 反応物 | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetyl chloride | HCID 21474483 | — |
| 生成物 | Allyl 4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoate | HCID 53900024 | — |
反応手順
In a manner similar to Example l(d), by reaction of 4.5 g (16.8 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl -2-naphthylacetyl chloride with 3 g (16.8 mmol) of allyl 4-aminobenzoate, 5.1 g (75%) of the expected ester are obtained in the form of a slightly yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05439925 |
| 出典データセット | uspto-grants-1995_08 |
| ORD ID | ord-49ee10be24a94b698a5a294bd90e4683 |
| 出典メモ | uspto-grants-1995_08 |