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5-methoxy-1-methyl-1H-indole-3-carbaldehyde → 1-(5-Methoxy-1-methyl-1H-indol-3-yl)-N-methylmethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-methoxy-1-methyl-1H-indole-3-carbaldehyde | HCID 925973 | — |
| 反応物 | 1,3-dimethyl-1H-indole-2-carbaldehyde | HCID 2771468 | — |
| 反応物 | Methyl 2-((5-bromopyridin-2-yl)amino)acetate | HCID 22139049 | — |
| 生成物 | 1-(5-Methoxy-1-methyl-1H-indol-3-yl)-N-methylmethanamine | HCID 12283882 | 98% |
反応手順
According to the procedure of Preparation 13 (c), except substituting 5-methoxy-1-methyl-1H-indole-3-carboxaldehyde for the 1,3-dimethyl-1H-indole-2-carboxaldehyde, the title compound (0.85 g, 98%) was obtained as a light yellow oil: MS (ES) m/e 205.2 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741339B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-a0a8d5a420004846b85b90df8251267c |
| 出典メモ | uspto-grants-2010_06 |