化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 3,4-Diphenyl-1,2,5-thiadiazole-1,1-dioxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Benzil | HCID 8651 | — |
| 反応物 | Sulfamide | HCID 82267 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3,4-Diphenyl-1,2,5-thiadiazole-1,1-dioxide | HCID 11000109 | 84,416% |
反応手順
Hydrogen chloride is bubbled through a solution of benzil (24 g, 0.11 mmol) and sulfamide (11 g, 0.11 mmol) in methanol (120 mL) for 2 h followed by heating to reflux for 2 h. The reaction mixture is cooled to RT, and the precipitate that formed is filtered to give 25.1 g of the product 14.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741493B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-569fc833732c40199d9273c5321e5ed8 |
| 出典メモ | uspto-grants-2010_06 |