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Dibutylamine → 3-(Dibutylamino)-7-(dipropylamino)phenothiazin-5-ium iodide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dibutylamine | HCID 8148 | — |
| 反応物 | HCID 178457153 | HCID 178457153 | — |
| 生成物 | 3-(Dibutylamino)-7-(dipropylamino)phenothiazin-5-ium iodide | HCID 178449028 | — |
反応手順
This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with dibutylamine. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C26H38N3OS requires m/z=424; found m/z=424 (I− not detected by mass spectrometry).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08188074B2 |
| 出典データセット | uspto-grants-2012_05 |
| ORD ID | ord-21ca49f3d77f49d3a5f03c77fbd3cf54 |
| 出典メモ | uspto-grants-2012_05 |