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tert-Butyl 4-oxopiperidine-1-carboxylate → tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| 反応物 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
| 生成物 | tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate | HCID 59333733 | 48% |
反応手順
tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate (285 mg, 48%) was synthesised from tert-butyl 4-oxopiperidine-1-carboxylate and 3-(3-fluorophenyl)propanoyl chloride according to the general procedure for the preparation of diketones. MS (ES+) m/z 250 (M+H)+
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08188101B2 |
| 出典データセット | uspto-grants-2012_05 |
| ORD ID | ord-41125c7fb85541a8968bc3f605dc388a |
| 出典メモ | uspto-grants-2012_05 |