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glucosamine tetra-O-acetate → 2-nitro-4-[3',5'-bis(ethyl)-2',4',6'-triiodophenyl]-benzoyl-1,3,4,6-tetra-O-acetyl-D-glucosamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | glucosamine tetra-O-acetate | HCID 13059363 | — |
| 反応物 | 2',4',6'-Triiodo-3',5'-bis(ethyl)-3-nitrobiphenyl-4-carbonyl chloride | HCID 22342002 | — |
| 生成物 | 2-nitro-4-[3',5'-bis(ethyl)-2',4',6'-triiodophenyl]-benzoyl-1,3,4,6-tetra-O-acetyl-D-glucosamine | HCID 86583522 | — |
反応手順
1,3,4,6-tetra-O-acetyl-D-glucosamine (9) is reacted with 2′,4′,6′-triiodo-3′,5′-bis(ethyl-3-nitrobiphenyl-4-carbonyl chloride (19) to yield 2-nitro-4-[3′,5′-bis(ethyl)-2′,4′,6′-triiodophenyl]benzoyl-1,3,4,6-tetra-O-acetyl-D-glucosamine (20).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06226352B1 |
| 出典データセット | uspto-grants-2001_05 |
| ORD ID | ord-5cd3c3d8210940eeb6cfa6a1937f37d8 |
| 出典メモ | uspto-grants-2001_05 |