化工社化工社 化学情報印刷レポート · 研究参考用
3-azetidinecarboxylic Acid → 1-{5-[4-(2-Isopropyl-phenoxy)-benzylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-azetidine-3-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-azetidinecarboxylic Acid | HCID 93192 | — |
| 反応物 | 5-[4-(2-Isopropyl-phenoxy)-benzylidene]-2-methylsulfanyl-thiazol-4-one | HCID 69089929 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 1-{5-[4-(2-Isopropyl-phenoxy)-benzylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-azetidine-3-carboxylic acid | HCID 69090386 | — |
反応手順
was prepared from 5-[4-(2-Isopropyl-phenoxy)-benzylidene]-2-methylsulfanyl-thiazol-4-one and azetidine-3-carboxylic acid and substituting MeCN with DMF as described in Example 5C
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08580832B2 |
| 出典データセット | uspto-grants-2013_11 |
| ORD ID | ord-0a181029bd3b42d4bbd01523928417cf |
| 出典メモ | uspto-grants-2013_11 |