化工社化工社 化学情報印刷レポート · 研究参考用
Piperonal → Bis(3,4-methylenedioxy)chalcone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperonal | HCID 8438 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Acetopiperone | HCID 76622 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Bis(3,4-methylenedioxy)chalcone | HCID 294346 | — |
反応手順
A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09051253B2 |
| 出典データセット | uspto-grants-2015_06 |
| ORD ID | ord-f07f4bc4c5814b05824736c9efcf4768 |
| 出典メモ | uspto-grants-2015_06 |