Triethyloxonium tetrafluoroborate → Ethyl 4-chloro-2-fluorobenzimidate

HRID 2232456

反応式

HRID 2232456 の反応式
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[O:7])=[C:4]([F:11])[CH:3]=1.F[B-](F)(F)F.[CH2:17]([O+](CC)CC)[CH3:18]>>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](=[NH:8])[O:7][CH2:17][CH3:18])=[C:4]([F:11])[CH:3]=1

参加物

3

反応物 2

HCID 2723982Triethyloxonium tetrafluoroborateHCID 37218494-Chloro-2-fluorobenzamide

生成物 1

HCID 19373098Ethyl 4-chloro-2-fluorobenzimidate

実験手順

starting from 4-chloro-2-fluorobenzamide and triethyloxonium tetrafluoroborate there is obtained ethyl 4-chloro-2-fluorobenzimidate as an oil; mass spectrum: 202 (3.5), 201 (1), 200 (10), 182 (2), 173 (27), 157 (100), 156 (75);

出典と根拠

ORDレコード
ord-9015969e3d704a7ca5621d033eedd6d4
出典データセット
uspto-grants-1988_11
特許番号
US04788210

関連ノート

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