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3-Tert-butyl-4-methoxybenzoyl chloride → Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Tert-butyl-4-methoxybenzoyl chloride | HCID 13633555 | — |
| 反応物 | Allyl 4-hydroxymethyl-2-hydroxybenzoate | HCID 21474558 | — |
| 生成物 | Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate | HCID 21474526 | — |
反応手順
In a manner similar to Example 1(d), by reaction of 2.4 g (10.5 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 2.2 g (10.5 mmol) of allyl 4-hydroxymethyl-2-hydroxybenzoate, 2.5 g (61%) of the expected allyl ester are obtained in the form of a slightly yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05688817 |
| 出典データセット | uspto-grants-1997_11 |
| ORD ID | ord-3fd2230ffb6d4043807846fb672aac58 |
| 出典メモ | uspto-grants-1997_11 |