化工社化工社 化学情報印刷レポート · 研究参考用
Acetone → 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | 3-Bromo-1,2-propanediol | HCID 20827 | — |
| 反応物 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 生成物 | 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane | HCID 169759 | — |
反応手順
An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04851502 |
| 出典データセット | uspto-grants-1989_07 |
| ORD ID | ord-137e2323cbb8440bab45f00bb57fe83c |
| 出典メモ | uspto-grants-1989_07 |