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Propionic Acid → Manganese dipropionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propionic Acid | HCID 1032 | — |
| 反応物 | Manganese carbonate | HCID 11726 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Manganese dipropionate | HCID 12054679 | 80% |
反応手順
In a reaction vessel, 145.83 grams of manganese carbonate, 328.92 grams of propionic acid and 25.38 grams of sodium hydroxide, a relative molar ratio of 2:7:1 respectively, was combined and heated to reflux. Water was removed from the vessel during the reaction by means of a fractional distillation column. The reaction went to completion after 10 hours, producing a dark burgundy solution from which about 80 percent of the remaining acid was removed. The product solidified at 130° C. The final product contained 80.7 percent manganese propionate and 19.3 percent sodium propionate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05591878 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-3162a71195424690b6cabb0ba3f2f8a5 |
| 出典メモ | uspto-grants-1997_01 |