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Phenylhydrazine → HCID 178515184、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylhydrazine | HCID 7516 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Ethyl 4-Chloroquinoline-3-carboxylate | HCID 268963 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | HCID 178515184 | HCID 178515184 | — |
反応手順
A suspension of ethyl 4-chloro-quinoline-3-carboxylate (3a) (2.35 g, 0.01 M) in 20 mL of o-xylene was refluxed with triethylamine (2.0 mL, 0.02 M) and phenyl hydrazine (2.89 g, 0.02 M) overnight. The crude product was obtained by filtration followed by washing the solid with cold methanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07863266B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-14d96c75fdcb4a85a34f10dc3a1a4f64 |
| 出典メモ | uspto-grants-2011_01 |