化工社化工社 化学情報印刷レポート · 研究参考用
2,4-Difluorobenzenesulfonyl Chloride → HCID 178484849、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4-Difluorobenzenesulfonyl Chloride | HCID 2734273 | — |
| 反応物 | HCID 178484847 | HCID 178484847 | — |
| 生成物 | HCID 178484849 | HCID 178484849 | — |
反応手順
In analogy to example 11.9, trans-[4-(4-Bromo-butoxy)-cyclohexyl]-methyl-amine hydrochloride and 2,4-difluoro-benzenesulfonyl chloride (with 2.1 eq N,N-diisopropylethylamine) were reacted to yield trans-N-[4-(4-Bromo-butoxy)-cyclohexyl]-2,4-difluoro-N-methyl-benzenesulfonamide which was used directly in the next steps see Example 12.57-12.58 and 12.65 and 12.66.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-a880bc35e718474580a8d818afe49a92 |
| 出典メモ | uspto-grants-2005_02 |