化工社化工社 化学情報印刷レポート · 研究参考用
Diethyl Malonate → Diethyl 2-[(1-tridecynyl)phenyl]methylenepropan-1,3-dioate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethyl Malonate | HCID 7761 | — |
| 反応物 | 2-(1-Tridecynyl)benzaldehyde | HCID 13688501 | — |
| 生成物 | Diethyl 2-[(1-tridecynyl)phenyl]methylenepropan-1,3-dioate | HCID 20165387 | — |
反応手順
A solution of 2-(1-tridecynyl)benzaldehyde (6.42, 22.6 mmol from example 3) was condensed with diethyl malonate (3.72 g) as described in example 1 to give 2.00 g (21%, 36% on the basis of unrecovered starting material) of the title compound identical with that prepared in example 6 above.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04699995 |
| 出典データセット | uspto-grants-1987_10 |
| ORD ID | ord-62f05dd6140a4f23af3c4f8e6bc03328 |
| 出典メモ | uspto-grants-1987_10 |