関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Potassium Nitrate | HCID 24434 | — |
| 反応物 | N-(3-formylphenyl)acetamide | HCID 256849 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | N-(3-formyl-4-nitrophenyl)acetamide | HCID 13987601 | 48.8% |
反応手順
A solution of potassium nitrate (6.2 g, 61 mmol) in sulfuric acid (30 mL) was added dropwise to stirred solution of N-(3-formylphenyl)acetamide (10.0 g, 61 mmol) in sulfuric acid (120 mL) maintained at 5° C. After 2 hours, the reaction mixture was poured onto ice water (500 mL) and filtered to give N-(3-formyl-4-nitrophenyl)acetamide (6.2 g, 48%) mp 131°-135° C., used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04701459 |
|---|
| 出典データセット | uspto-grants-1987_10 |
|---|
| ORD ID | ord-d972c48809d24f6790d4889bc1c8c1e7 |
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| 出典メモ | uspto-grants-1987_10 |
|---|
