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4-Iodoaniline → N-(4-iodophenyl)-N-methylethanesulphonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Iodoaniline | HCID 10893 | — |
| 反応物 | Ethanesulfonyl chloride | HCID 11667 | — |
| 反応物 | N-(4-iodophenyl)methanesulfonamide | HCID 836147 | — |
| 生成物 | N-(4-iodophenyl)-N-methylethanesulphonamide | HCID 19785600 | — |
反応手順
The product so obtained was used in place of 4-iodoaniline in the procedure described in Example 3 for the preparation of N-(4-iodophenyl) methanesulphonamide and ethanesulphonyl chloride was used in place of methanesulphonyl chloride. Thus was obtained N-(4-iodophenyl)-N-methylethanesulphonamide as an oil. NMR Spectrum 1.45 (3H, t), 3.00 (2H, q), 3.35 (3H, s), 7.15 (2H, m), 7.70 (2H, m).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05258399 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-5611fef512954a2ea8368584f719a99e |
| 出典メモ | uspto-grants-1993_11 |