化工社化工社 化学情報印刷レポート · 研究参考用
Dibutylcarbamoyl chloride → 1,1-Dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dibutylcarbamoyl chloride | HCID 83371 | — |
| 反応物 | 4,5,6,7-Tetrahydro-1-benzothiophen-4-amine | HCID 4216372 | — |
| 生成物 | 1,1-Dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea | HCID 20348947 | — |
反応手順
Similarly, diethyl-, dipropyl-, and dibutylcarbamoyl chloride are reacted with 4,5,6,7-tetrahydrobenzo[b]thiophen-4-amine to afford 1,1-diethyl-, 1,1-dipropyl-, and 1,1-dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea, respectively. Substitution of the above-mentioned carbamoyl chlorides with the corresponding thiocarbamoyl chlorides affords the corresponding thioureas.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04036979 |
| 出典データセット | uspto-grants-1977_07 |
| ORD ID | ord-9a432fcd75d641c58cc0b0316a280d0e |
| 出典メモ | uspto-grants-1977_07 |