化工社化工社 化学情報印刷レポート · 研究参考用
2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → N-[(1R,2R)-2-cyclohexylcyclopentyl]piperidin-2-imine;hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- | HCID 75657 | — |
| 反応物 | o-Methylvalerolactim | HCID 138567 | — |
| 反応物 | cis-2-Cyclohexylcyclopentylamine hydrochloride | HCID 70050481 | — |
| 反応物 | rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride | HCID 70051154 | — |
| 生成物 | N-[(1R,2R)-2-cyclohexylcyclopentyl]piperidin-2-imine;hydrochloride | HCID 145795656 | — |
反応手順
Following the procedure of Example 1, only substituting for cis-2-phenylcyclopentylamine hydrochloride and O-methylcaprolactim, appropriate amounts of cis-2-(cyclohexyl)cyclopentylamine hydrochloride and O-methylvalerolactim respectively the desired product was obtained. M.P. 195.5°-197° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04153235 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-dd6c3bce4f6d4061ae5e6c21df4adbfc |
| 出典メモ | uspto-grants-1979_05 |