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Potassium Carbonate → 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Nafimidone monohydrochloride | HCID 51199 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone | HCID 51200 | — |
反応手順
1-(2-Naphthoylmethyl)imidazole hydrochloride (1.0 g.) suspended in 50 ml. of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-(2-naphthoylmethyl)imidazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04150153 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-db5c8d01e01c4b6882b725e1358bba66 |
| 出典メモ | uspto-grants-1979_04 |