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3,4-dihydro-2H-pyran → HCID 19032980、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-dihydro-2H-pyran | HCID 8080 | — |
| 反応物 | 4-Aminobutyric acid methyl ester hydrochloride | HCID 2756383 | — |
| 反応物 | 2-(4-Chlorobenzenesulfonamido)-3-hydroxypropanoic acid | HCID 4229170 | — |
| 生成物 | HCID 19032980 | HCID 19032980 | — |
反応手順
The procedure described in Example 1 was repeated, except that dihydropyran (1.37 ml) and methyl 4-aminobutanate hydrochloride (1.69 g) were successively reacted with (RS)-2-(4-chlorobenzenesulfonylamino)-3-hydroxypropanoic acid (2.80 g) to obtain (RS)-2-(4-chlorobenzenesulfonylamino)-N-(3-methoxycarbonylpropyl)-3-(tetrahydropyran-2-yloxy)propanamide (3.12 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05650428 |
| 出典データセット | uspto-grants-1997_07 |
| ORD ID | ord-676d72dcd94740218f1078993540da1c |
| 出典メモ | uspto-grants-1997_07 |