化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Methyl 3-(sec-butylcarbamoyl)acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 3-(Sec-butylcarbamoyl)acrylic acid | HCID 244595 | — |
| 生成物 | Methyl 3-(sec-butylcarbamoyl)acrylate | HCID 54128810 | — |
反応手順
To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07449242B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-4c7dd66728e1478c8e5011a149f328cd |
| 出典メモ | uspto-grants-2008_11 |