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4-Ethylbenzoic Acid → 4-Ethylbenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylbenzoic Acid | HCID 12086 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | 4-Ethylbenzoyl chloride | HCID 85368 | — |
反応手順
200 g (1.33 millimoles) of 4-ethylbenzoic acid are added rapidly to 500 ml of thionyl chloride with stirring. The mixture is heated at the reflux temperature for 4 hours. After evaporation of the SOCl2 and distillation, 4-ethylbenzoyl chloride is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04588748 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-26a1f02e2dba46d39f0ba1c267c7aba8 |
| 出典メモ | uspto-grants-1986_05 |