化工社化工社 化学情報印刷レポート · 研究参考用
Phenylglyoxal → N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-phenylethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylglyoxal | HCID 14090 | — |
| 反応物 | 3-(4-Methylphenyl)propan-1-amine | HCID 12564270 | — |
| 生成物 | N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-phenylethanamine | HCID 20212420 | — |
反応手順
The title compound was prepared in the manner described in Example 9 using phenylglyoxal and 3-(4-Methylphenyl)propanamine. Recrystallization of the chromatographed material from benzene-hexane gave the title compound m.p. 114-116. τ(CDCL3) 8.15 (2H, m), 7.7 (3H, s), 6.9-7.5 (6H, m+2H, disappears with D2O), 5.3 (1H, m), 2.9 (4H, s), 2.7 (5H, m).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04588749 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-ee42504e3d654a9b9c7dea16de494dc3 |
| 出典メモ | uspto-grants-1986_05 |