化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Phenanthrenedione → 1,2-Naphthoquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Phenanthrenedione | HCID 3080566 | — |
| 反応物 | Alpha-Ionone | HCID 5282108 | — |
| 生成物 | 1,2-Naphthoquinone | HCID 10667 | — |
反応手順
In order to test and evaluate the equipment and methods of the present invention, pre-coated 10 cm×10 cm HPTLC plates (Whatman) and test compounds α-ionone, phenanthrenequinone and 1,2-naphthaquinone (Aldrich) were obtained. The test compounds were initially diluted with acetone to about 10 mg/ml and stock solutions stored below 4° C. The stock solutions were further diluted with acetone just before use. Ceric sulfate prepared by adding 42 g of (NH4)4Ce(SO4)4 and 56 ml of conc. H2SO4 in 1 liter of distilled water was the chromogenic reagent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04591272 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-c0c231f249374e189fbc6c34c3d16dc3 |
| 出典メモ | uspto-grants-1986_05 |