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化工社化工社 化学情報印刷レポート · 研究参考用
HRID 280798作成日:2026年10月24日

1,2-Phenanthrenedione → 1,2-Naphthoquinone

https://huagongshe.com/ja/reaction/280798

反応式

関与物質

役割名称HCID仕込み量
反応物1,2-PhenanthrenedioneHCID 3080566—
反応物Alpha-IononeHCID 5282108—
生成物1,2-NaphthoquinoneHCID 10667—

反応手順

In order to test and evaluate the equipment and methods of the present invention, pre-coated 10 cm×10 cm HPTLC plates (Whatman) and test compounds α-ionone, phenanthrenequinone and 1,2-naphthaquinone (Aldrich) were obtained. The test compounds were initially diluted with acetone to about 10 mg/ml and stock solutions stored below 4° C. The stock solutions were further diluted with acetone just before use. Ceric sulfate prepared by adding 42 g of (NH4)4Ce(SO4)4 and 56 ml of conc. H2SO4 in 1 liter of distilled water was the chromogenic reagent.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04591272
出典データセットuspto-grants-1986_05
ORD IDord-c0c231f249374e189fbc6c34c3d16dc3
出典メモuspto-grants-1986_05